Chemical Analysis Automation
The Chemical Analysis Automation (CAA) ProgramΖs objective is to promote the development and commercialization of chemical analysis and sample preparation technologies necessary for the automation of DOE and private contract environmental laboratories. This effort is in direct response to the tremendous need for chemical characterization of contaminated environmental soil samples, contents of storage tanks, water samples, and other sample matrices under the control of DOE that must take place before remediation can be initiated. The technologies being developed by the CAA team have additional value as commercial products for other chemical applications and laboratories involved in other markets, such as petro-chemical, food and flavorings, cellulose, polymers, and mining. The CAA team has made substantial progress towards its goal of automating the environmental analytical laboratory under a standardized and modular paradigm known as the Standard Analysis Method (SAM). The first system, the organic system for PCB analysis in soils has been integrated and tested. To date, a suite of 14 Standard Laboratory Modules (SLM ), the backbone of this integrated technology, has been designed and developed. Also, several detailed surveys of the environmental market and its needs were commissioned to help focus and prioritize development.
No image. Developers:
•  Los Alamos National Laboratory Idaho National Engineering & Environmental Laboratory Oak Ridge National Laboratory
Applications:
•  Rapid automated analysis of solid waste samples at PCB-contaminated sites such as Oak Ridge Paducah WAG 23, Idaho, Hanford
•  Analysis of a broad range of organic contaminants at cleanup sites across DOE
Benefits:
•  30-50% reduction in sample analysis costs
•  Rapid sample turnaround times; reducted data variability
•  Minimized human exposure; improved analyst safety
•  Reduction in analytical laboratory pollution
•  Increased sample throughput
Status:
•  Prototype modules for the GC System have been developed and demonstrated to gain both operational experience and user acceptance.
•  Between FY98 and FY00, prototypes of successive systems are planned in parallel with the commercial deployment/market introduction
•  Commercialization partner: Advanced Power Technologies, Inc.
•  See Technology #s 2069, 2070, 2071, 2072, 2075, & 2077
Milestones: 
Completed
Incomplete
PR
FY 97
DP     AI     DM
FY 98
  IT - ITSR Publication; PR - Peer Review; DP - Deployment; AI - Available for Implementation; DM - Demonstration; BST - Bench-Scale Testing;
9/19/02 Characterization, Monitoring and Sensor Technology OST Ref #: 72